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Harry
O'Neil Brotherton, Jr.
ADDRESS: Office Phone: (318)342-1829
E-mail: hbrotherton@ulm.edu
EDUCATION:
Master
of Science - University
of Tennessee. August, 1976. Thesis: "Fourier Transform Infrared Spectroscopy of
Selected Polycyclic
Aromatic Hydrocarbons Using Conventional Sampling Techniques," with G.
Mamantov and E. L. Wehry.
Bachelor
of Arts - Pfeiffer
College. May, 1973. Major: Chemistry; Minor: History.
PROFESSIONAL EXPERIENCE:
Head, Department of Chemistry,
University of Louisiana at Monroe, Fall 2001 - Fall 2009.
Associate
Professor, University
of Louisiana at Monroe, Fall 1987 - 2004.
Assistant
Professor, Northeast
Louisiana University, Fall 1982 - 1987.
Instructor, University of
Tennessee-Chattanooga. Spring 1978.
Instructor, University of Tennessee. Fall 1976
- Fall 1977.
ACTIVITIES:
Member : American Society for Mass Spectrometry
Member : Louisiana Academy of Sciences
Member : Sigma Xi
Officer : Ouachita Valley Section of the ACS; Secretary-Treasure, 1986;
Chair-Elect, 1987-88; Chairman, 1988-89; Councilor, 1989-2004.
Member : ACS AN94 analytical examination committee
Member : ULM Graduate Council, 1992 to 2004
Chair : ULM Graduate Council, 2001 to 2004
Graduate Coordinator for the College of Pure and Applied Sciences, 1992
to 2002
Monroe Jaycees' "Young Educator of the Year-1983"
Co-instructor: "Advances in Mass Spectroscopy" short course at FACSS in
Philadelphia, Fall, 1983.
PUBLICATIONS:
"Determination of Drugs in Blood Serum by Mass Spectrometry/Mass
Spectrometry", (with R. A. Yost). Anal.
Chem.,55(3),549-553(1983).
"Tandem Mass Spectrometry for Studies of Drug Action and Metabolism",
(with R. A. Yost and R. J. Perchalski).
Int.
J. Mass Spectrom. Ion Phys.
, 48,77-80(1983).
"Pharmaceutical and Clinical Analysis by Tandem Mass Spectrometry", (with
R. A. Yost, R. J. Perchalski, J. V. Johnson, and M. B. Budd).
Talanta,31(10B), 929-935 (1984).
"Rapid Screening and Confirmation for Drugs and Metabolites in Racing
Animals by Tandem Mass Spectrometry", (with R. A. Yost). Am.
J.
Vet.
Res. , 45(11),2436-2440(1984).
"Triple Quadrupole MS/MS in Biomedical Research", (with J. V. Johnson, M.
S. Lee, M. R. Lee, and R. A. Yost) in Mass
Spectrometry in
Biomedical
Research.1986.
"Effect of Menthol and Related Terpenes on the Percutaneous Absorption of
Propranolol Across Excised Hairless Mouse Skin" (with J. R.
Kunta, V. R. Goskonda, M. A. Khan, and I. K. Reddy) in Journal
of Pharmaceutical Science, 86,1369(1997).
"A Solid Phase Extraction of Pesticides with Determination by Gas
Chromatography" (with A. Bhuiyan) in Journal
of the Arkansas Academy
of
Science, 56,18(2002).
"Facile Access to Novel Organotellurium Heterocycles by Nitration of
Bis(3,5-Dimethylphenyl)Ditelluride" (with P. R. Mallikarachy, F. R.
Fronczek, and T. Junk) in J.
Heterocycl. Chem.,
42,243-247(2005).
MS THESES DIRECTED:
"Studies of Selected Steroids by Thermospray LC/MS/MS", Sandra Lee Green,
December, 1986.
"Analysis of Selected Pesticides by GC/MS/MS", Nalinee Phanawat, May,
1987.
"The Effect of varying Collision Energy and Collision Gas Pressure on the
Fragmentation of Selected Molecules in Triple Quadrupole Mass
Spectrometry", Stanley Hudnall, August, 1987.
"Solid-phase Extraction and Thermospray LC/MS/MS for the Detection of
Selected Anabolic Steroids and their Metabolites",
Kathleen
Anderson, August, 1989.
"Analysis of Commercial Fumaric Acid Samples by High Performance
LiquidChromatography (HPLC)", Dasheng Chu, August, 1990.
"The Concentration of Selected Metals in Paper Food Packaging", Jian
James Xu, December, 1990.
"Solid Phase Extraction and Thermospray LC/MS/MS for the Detection of
Marijuana and its Major Metabolite", Mohammad Ghazizadeh,
December, 1990.
"Analysis of Centennial Variety Soybean Foliage by Gas
Chromatography/Mass Specrtometry", Helene Weber, May, 1992.
"Chlorinated Pesticide and PCB Concentrations in the White Tailed Deer
(Odocoileus Virginianus) from Northeast Louisiana", Mario
Fernandez, May, 1992.
"Rapid Clean Up of Fat Extracts For Pesticide Determinations Using
Solid-Phase (C-18) Extraction Disks", Shubada Kulkarni,
December, 1993.
"Solid Phase Extraction of Pesticides from Water with Determination by
Gas Chromatography", Anwarul Bhuiyan, May, 1994.
"Solid Phase Extraction of Pesticide Residues from Ground Water",
Shailesh Kulkarni, May, 1995.
"Rapid Clean Up by Acetone Cold Precipitation and C18 Solid-Phase
Extraction of Pesticides in Meat Samples", Yanyun Chen, May, 1995.
"Solid Phase Extraction of Pesticides Residues from Ground Water with
Determination by Gas Chromatography", Haiqun Liu, August, 1996.
"Determination of Heavy Metals in Fish By Atomic Absorption
Spectroscopy", Junge Zhang, May, 1997.
"Pesticide Residue Determinations from Fish Tissue", Regina Stencil,
December, 1997.
“Determination of Lead in Fish by Atomic Absorption Spectroscopy", Min
Xiao, December, 1998.
"Determination of Trace Levels of Pesticides in Surface Water From
Northeast Louisiana", Hua Zhao, December, 1998.
"Comparison of Selected Detectors for the Determination of Pesticides in
Crayfish", Anita Dalvi, August, 2000.
PAPERS PRESENTED
Reference Materials for Oil Shale Processing, NBS, Gaithersburg, MD,
November, 1975.
"Screening for Drugs and Metabolites in Racing Animals by
TripleQuadrupole MS/MS", (with R. A. Yost) Pittsburgh Conference
on
Analytical Chemistry and Applied Spectroscopy, Atlantic City, NJ,
1982.
"Trace Analysis of Drugs and Metabolites in Physiological Tissues by
Tandem Mass Spectrometry", (with R. J. Perchalski and R. A. Yost)
ACS National Meeting, Las Vegas, NV, April, 1982.
Tandem Mass Spectrometry for Studies of Drug Action and Metabolism",
(with R. J. Perchalski and R. A. Yost) 30th Annual Conference on
Mass Spectrometry and Allied Topics, Honolulu, May, 1982.
"Tandem Mass Spectrometry for Studies of Drug Action and Metabolism",
(with R. J. Perchalski and R. A. Yost) 9th International
Mass
Spectrometry Conference, Vienna, August, 1982.
"The Use of Triple Quadrupole Mass Spectrometry (MS/MS) in Drug
Analysis", Invited Speaker, Fifth International Conference: Control of
Use of Drugs in Race Horses, Toronto, Canada, June, 1983.
"Tandem Mass Spectrometry for Trace Analysis of Drugs in Biological
Fluids", (with R. A. Yost) LA Academy of Sciences, New Orleans,
1984.
"Determination of Heavy Metal Levels in Edible Fish Tissue", (with J.
Zhang) LA Academy of Sciences, Alexandria, 1997.
"An Evaluation of Lead Levels In Edible Fish Tissue", (with J. Zhang and
Min Xiao) LA Academy of Sciences, Monroe, 1999.
"Comparison of GC/MS, GC/ECD, GC/TSD, and HPLC/UV for the Analysis of
Organochlorine and Organophosphate Pesticides", (with A.
Dalvi) LA Academy of Sciences, Shreveport, 2000.
"Mercury Levels in Crayfish", (with T. Junk and M. Godwin) LA Academy of
Sciences, Shreveport, 2000.
"The Analysis of Mercury Levels in Human Breast Milk", (with R. M.
Childress) Second Annual Student Research Symposium, University of
Louisiana at Monroe, Monroe, LA, April, 2002.
"Solid Phase Extraction of Pesticides with Determination by Gas
Chromatography", (with Anwar Bhuiyan) Arkansas Academy of Sciences,
Little Rock, AR, April, 2002.
PROPOSALS:
"Enhancement of Instrumental Analysis Facilities", $70,000, LEQSF,
1996-7.
"Chemical Science and Technology Courses at NLU", with Dr. F. Watson,
LEQSF, $25,000, 1996-7.
"Modernization of NLU's Instrumental Teaching Laboratory", with Dr. T.
Junk, BORSF, $59,070, 1999-2000.
"Acquisition of a Mass Spectrometer for Undergraduate Laboratories and
Research", with Dr. Jim Plamer, Dr. Frank Ji, Dr. Dale Snow,
Dr. Upali Siriwardane, BORSF, $94,635, 2002-2003.
"Upgrading ULM's Instrumental Teaching Capabilities", with Dr. T. Junk,
BORSF, $68,106, 2002-2003.
"Acquisition of a Mass Spectrometer for Undergraduate Laboratories and
Research”, with Dr. Jim Palmer, Dr. Frank Ji, Dr. Dale Snow, and
Dr. Upali Siriwardane, $84,635, BORSF, 2002-03.
“Acquisition of an Inductively Coupled Plasma Optical Emission
Spectrometer (ICP-OES)”, with Thomas Junk, Danny Hubbard,
Pia Alburquerque, $90,683.00 ($20,000 ULM match), BORSF,
2004-05.
“Triple-Quadrupole HPLC-MS/MS System for Enhancement of Pharmaceutical
Sciences, Chemistry, and Toxicology Research at ULM”,
with
Ronald Hill, Khalid El Sayed, Harihara M. Mahendale, Melgardt de Villiers,
Sharon Meyer, Kevin Baer, William Kolling, and
Sami Nazzal, $193,550 ($80,000 ULM match), BORSF, 2004-05.
“Using Inquiry based Instruction in Chemistry Laboratory Courses”, with
Pia Alburquerque, Bobby Burkes, and Danny Hubbard,
$195,911.00, NSF-CCLI, 2004-05.
“Enhancement of General Chemistry Laboratory Capabilities”, $30,000, ULM
STAP Funds, Spring 2006.
“Introduction of Microwave Assisted Techniques to ULM’s Chemistry
Program”, with Thomas Junk. $81,060 ($20,000 ULM Match),
BORSF, Submitted Fall 2007. |